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SAXS instrument
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SAXS instrument

Instrument scientists:
Dr Tracey Hanley (Responsible officer)
Dr Robert Knott

See the SAXS instrument schedule

Description

A Small Angle X-ray Scattering (SAXS) instrument has been installed in the guide hall at OPAL. The SAXS instrument is a Bruker Nanostar equipped with a rotating anode source and three-pinhole collimation. SAXS is complimentary to Small Angle Neutron Scattering (SANS) which will be available on the new QUOKKA instrument at the OPAL reactor. A variety of sample environments are available for solids and liquids, including two temperature control units one covering temperature range -30oC to 120oC and a second unit for ambient to 300oC. The instrument is capable of being run in two separate configurations either high resolution or high flux; the q-range accessible is 0.005 A-1 to 3.1 A-1 in high resolution mode and 0.01 A-1 to 3.1 A-1 in high flux mode.

Applications

SAXS is used to study any materials with structure of the length scale 1-100nm. The performance of many advanced materials is crucially dependent on nanostructure, and SAXS can be used to study this. It can be used for study of density variations, colloidal sizes, particles sizes, porosity, domain sizes, orientation, phase identification, the list is endless. With research being directed more towards nano-sized science, SAXS is becoming a widely used tool.

Instrument Specifications

Rotating Anode Cu Ka source (1.541 A)
Cross-coupled Gobel mirrors
3 pinhole collimation
Large multifunctional sample chamber
Sample temperature control from -30oC to 150oC or ambient to 300oC
Hi-Star 2D detector with 100µm resolution
Capability of two configurations: high resolution or high intensity.
Qmin = 0.005 A-1
Qmax = 3.1 A-1

Example Data

Silver Behenate
rat tail collagen
Silver Behenate
Rat Tail Collagen
High Density Polyethylene
Water
High Density Polyethylene
Water

Instrument time is available for further information please click on links below:

click here for AINSE member institutes
click here for ANSTO users
Click here for Commercial users

See also the Small Angle Neutron Scattering (SANS) instrument